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The number sequence corresponds to increasing retention times and decreasing polarity of the metabolites after hydrolysis, but before acetylation. Deuterated TREN metabolites and diagnostic product ions (CE = 20 and CE = 30 eV) after hydrolysis of phase-II metabolites, HPLC fractionation and acetylation identified by LC-ESI-HRMS. Altogether, a total of 20 phase-II metabolites of relevant traceability was identified. Almost all metabolites were found to be eliminated as differently conjugated products including the well-characterized glucuronic acid and sulfate conjugates, as well as alkaline-labile phase-II metabolites. De-conjugation under alkaline conditions is less established for human metabolism, but has already been assessed in preventive doping research to generate cysteine conjugates (Fabregat et al, steroid eye drops pharmacy.
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